HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19096815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3,5-Dichloroaniline | HCID 12281 | — |
| Reactant | HCID 19096901 | HCID 19096901 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19096815 | HCID 19096815 | — |
Reaction Steps
In a manner similar to the procedure described-in Example I, 3,5-dichloroaniline was reacted with methyl chlorocarbonyl(dimethoxy)acetate, prepared as described in Example LXV Part A, employing triethylamine as the acid acceptor in methylene chloride solution. The methyl 3-[(3,5-dichlorophenyl)amino]-2,2-dimethoxy-3-oxopropanoate product (2.31 grams, 0.007 mole) was obtained as colorless crystals having a melting point of 160° C.-164° C. Elemental analysis of the product indicated the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292937 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-18e3d2ea4ee44e839af55d8543d0d272 |
| Source note | uspto-grants-1994_03 |