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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 487018Generated: October 27, 2026

Triethylamine → ethyl 1-[N-(4-bromophenyl)-N-methylaminocarbonyl]cyclopropanecarboxylate

https://huagongshe.com/reaction/487018

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantBenzenamine, 4-bromo-N-methyl-HCID 2757052—
ReactantEthyl 1-chlorocarbonylcyclopropanecarboxylateHCID 14233946—
Productethyl 1-[N-(4-bromophenyl)-N-methylaminocarbonyl]cyclopropanecarboxylateHCID 1909687050%

Reaction Steps

Ethyl 1-chlorocarbonylcyclopropanecarboxylate (3.11 grams, 0.02 mole), prepared in Example XVIII, 4-bromo-N-methylaniline (3.00 grams, 0.02 mole) and triethylamine (1.63 grams, 0.02 mole) were reacted in a manner similar to that described in Example III to give 3.79 grams (0.01 mole) of ethyl 1-[N-(4-bromophenyl)-N-methylaminocarbonyl]cyclopropanecarboxylate isolated as a colorless oil. Elemental analysis of the product indicated the following:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05292937
Source datasetuspto-grants-1994_03
ORD IDord-458f4868980f4b799d0a47d178c4f541
Source noteuspto-grants-1994_03