HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 19096830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3,5-Dichloroaniline | HCID 12281 | — |
| Reactant | Monoethylmethylmalonate | HCID 22667308 | — |
| Product | HCID 19096830 | HCID 19096830 | 10% |
Reaction Steps
Monoethyl methylmalonate (5.0 grams, 0.03 mole), 3,5-dichloroaniline (5.54 grams, 0.03 mole) and 1,3-dicyclohexylcarbodiimide (7.06 grams, 0.03 mole) were reacted in a manner similar to that described in Example LVII to give 1.0 gram (0.003 mole) of ethyl 2-(3,5-dichlorophenylaminocarbonyl)propanoate having a melting point of 89° C.-90° C. Elemental analysis of the product indicated the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292937 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-bf40a646d9854c51a890d6ef15f972c4 |
| Source note | uspto-grants-1994_03 |