HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 19096892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 85543209 | HCID 85543209 | — |
| Product | HCID 19096892 | HCID 19096892 | 30% |
Reaction Steps
3-Chloroaniline (2.82 grams, 0.02 mole), monoethyl methoxymalonate (3.58 grams, 0.02 mole), prepared in Example LIII Part B, and 1,3-dicyclohexylcarbodiimide (4.50 grams, 0.02 mole) were reacted in a manner similar to that described in Example LVII to give 1.60 grams (0.006 mole) of ethyl 3-[(3-chlorophenyl)amino]-2-methoxy-3-oxopropanoate having melting point of 43.5° C.-46.5° C. Elemental analysis of the product indicated the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292937 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-ec72106afd6b44b2acd7d7e629c66cbd |
| Source note | uspto-grants-1994_03 |