HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromohexanoic acid → 6-Bromohexanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromohexanoic acid | HCID 12013 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 6-Bromohexanoyl chloride | HCID 89848 | — |
Reaction Steps
58.5 g of (0.3 moles) of 6 bromohexanoic acid and 85 ml of oxalyl chloride are placed in a 250-ml flask with a magnetic agitator. The mixture is agitated and 1 milliliter of dimethylformamide (DMF) is added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05294463 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-b0c2c43ef3fd413fb7975f6bb0c6f238 |
| Source note | uspto-grants-1994_03 |