HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenesulfonyl chloride → HCID 19094007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenesulfonyl chloride | HCID 7404 | — |
| Reactant | HCID 19093897 | HCID 19093897 | — |
| Product | HCID 19094007 | HCID 19094007 | — |
Reaction Steps
The title compound was prepared by Method A using 2-(2-aminoethyl)-1,2,3,4-tetrahydroisoquinoline (described in Example 174) and 4-nitrobenzenesulfonyl chloride to produce the desired product in 98% yield. This material was crystallized from EtOAc to afford a gold-colored solid; mp 142.5°-144.5° C.; IR (KBr) 3372, 3110, 2778, 1929, 1603, 1521, 1305, 1151, 969 and 739 cm-.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05294621 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-e9a2c23c230145aeb3a36d4d88ceffb9 |
| Source note | uspto-grants-1994_03 |