HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tris(pentafluorophenyl)borane → Tris(pentafluorophenyl)borane hydrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tris(pentafluorophenyl)borane | HCID 582056 | — |
| Reactant | Borane, tris(pentafluorophenyl)-, trihydrate | HCID 11261567 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Tris(pentafluorophenyl)borane hydrate | HCID 15875499 | — |
Reaction Steps
A mixture of 0.566 gram (1 mmol) (C6F5)3B.3H2O as prepared in Example 1 and 1.024 grams (2 mmol) (C6F5)3B in 10 mL dichloromethane was stirred for 15 minutes and then evaporated to dryness under vacuum. A quantitative yield of the product remained and was stored under dry nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296433 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-1b827e7ec07d4899aeb5df2d140dad67 |
| Source note | uspto-grants-1994_03 |