HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 19092269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Reactant | 1-(4-Nitrophenyl)piperidin-4-one | HCID 3842562 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Product | HCID 19092269 | HCID 19092269 | — |
Reaction Steps
3.0 g (13.6 mmol) of 1-(4-nitrophenyl)-4-piperidone [cf. Taylor et al., Synthesis (1981) 606], 2.5 g (13.6 mmol) of N-(4-fluorophenyl)piperazine, 0.8 g (13.6 mmol) of acetic acid and 0.9 g (13.6 mmol) of sodium cyanoborohydride were reacted as in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296485 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-bb416e39ca754a29909dd4621d85c2a1 |
| Source note | uspto-grants-1994_03 |