HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57206089, compound → HCID 86747689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57206089 | HCID 57206089 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86747689 | HCID 86747689 | 89.1% |
Reaction Steps
To a solution of the product of Example 43 (28 mg) in methanol (10 ml) was added 10% Pd-on-C (5 mg) and the resulting suspension was then stirred in an atmosphere of hydrogen for 2 hours at 0° C. The reaction mixture was then filtered and volatiles were removed in vacuo. Chromatography on silica then gave the title compound as a foam (25 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296489 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-f909edd8aabf4230a1191e78ffb48abb |
| Source note | uspto-grants-1994_03 |