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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 487827Generated: October 31, 2026

HCID 57206089, compound → HCID 86747689, compound

https://huagongshe.com/reaction/487827

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57206089HCID 57206089—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86747689HCID 8674768989.1%

Reaction Steps

To a solution of the product of Example 43 (28 mg) in methanol (10 ml) was added 10% Pd-on-C (5 mg) and the resulting suspension was then stirred in an atmosphere of hydrogen for 2 hours at 0° C. The reaction mixture was then filtered and volatiles were removed in vacuo. Chromatography on silica then gave the title compound as a foam (25 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05296489
Source datasetuspto-grants-1994_03
ORD IDord-f909edd8aabf4230a1191e78ffb48abb
Source noteuspto-grants-1994_03