HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178437750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178437750 | HCID 178437750 | 63% |
Reaction Steps
This product is synthesised, in 63% yield, from 1,2,4-triazole and 1-vinyl-2-pyrrolidinone by a similar method described in Example 1. On account of the higher water solubility of this product, ethyl acetate (3×50 ml) is used to extract it from the aqueous phase during washing. The product distils as a pale yellow oil, bp 150°/0.05 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298178 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-a4081813d8af4fd6b9729984d110d713 |
| Source note | uspto-grants-1994_03 |