HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) → HCID 57069189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Reactant | (4S,5R)-5-Methyl-2-oxooxazolidine-4-carboxylic acid | HCID 11412450 | — |
| Product | HCID 57069189 | HCID 57069189 | 14.2% |
Reaction Steps
A procedure similar to that described in Example 19 was repeated, but using 180 mg of (4S,5R)-5-methyl-2-oxooxazolidine-4-carboxylic acid and 230 mg of N-(2-nitrooxyethyl)amine nitrate, after which the product was recrystallized from methylene chloride, to obtain 41 mg of the title compound as colorless needles, melting at 81.5°-82.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298516 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-2593a3da553c44a1b1404d889099471c |
| Source note | uspto-grants-1994_03 |