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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 488077Generated: October 30, 2026

Diethyl Ether → HCID 86745598, compound

https://huagongshe.com/reaction/488077

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
Reactant2-Naphthalenesulfonic acidHCID 8420—
ReactantHCID 54086927HCID 54086927—
ProductHCID 86745598HCID 86745598—

Reaction Steps

A 0.75 g portion of the cyclopropylaminoindole compound was dissolved in 75 ml Et2O and stirred while a solution of 0.69 g of 2-naphthalene sulfonic acid in 50 ml Et2O was added slowly. A white precipitate formed which was filtered under N2, washed with 2×50 ml Et2O and dried to afford 1.04 g of 4-methyl-1,2,3,4-tetrahydrocyclopent[b]indol-3-cyclopropylamine 2-naphthalene sulfonate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05298626
Source datasetuspto-grants-1994_03
ORD IDord-7c7b11bc7bb34c44a41d9a908b1d230d
Source noteuspto-grants-1994_03