HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 86745598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Naphthalenesulfonic acid | HCID 8420 | — |
| Reactant | HCID 54086927 | HCID 54086927 | — |
| Product | HCID 86745598 | HCID 86745598 | — |
Reaction Steps
A 0.75 g portion of the cyclopropylaminoindole compound was dissolved in 75 ml Et2O and stirred while a solution of 0.69 g of 2-naphthalene sulfonic acid in 50 ml Et2O was added slowly. A white precipitate formed which was filtered under N2, washed with 2×50 ml Et2O and dried to afford 1.04 g of 4-methyl-1,2,3,4-tetrahydrocyclopent[b]indol-3-cyclopropylamine 2-naphthalene sulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298626 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-7c7b11bc7bb34c44a41d9a908b1d230d |
| Source note | uspto-grants-1994_03 |