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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 488119Generated: October 30, 2026

5-Ethyl-3-methoxy-4-methoxymethoxy-1-naphthalenecarbaldehyde → 5'-Ethyl-3'-methoxy-4'-methoxymethoxy-1'-valeronaphthone

https://huagongshe.com/reaction/488119

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Ethyl-3-methoxy-4-methoxymethoxy-1-naphthalenecarbaldehydeHCID 9970569—
ReactantButyllithiumHCID 178418339—
SolventHexaneHCID 8058—
Product5'-Ethyl-3'-methoxy-4'-methoxymethoxy-1'-valeronaphthoneHCID 11724194—

Reaction Steps

5-Ethyl-3-methoxy-4-methoxymethoxy-1-naphthalenecarbaldehyde and a hexane solution of 1.6M n-butyl lithium were used and treated in the same manner as in Reference 6 to obtain the captioned compound as a yellow oily substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05298649
Source datasetuspto-grants-1994_03
ORD IDord-8028d947f6b34505a63ec51bc005ed88
Source noteuspto-grants-1994_03