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HRID488236

反应详情

EQUATION

反应方程式

HRID 488236 的结构方程式

REACTANTS

反应物

3
结构：O=S(=O)(Oc1ccccc1)C(F)(F)F
HCID548641

Phenyl trifluoromethanesulfonate

C7H5F3O3S

结构：CC[Si](CC)(CC)c1cc(C=O)co1
HCID10878438

3-Furancarboxaldehyde, 5-(triethylsilyl)-

C11H18O2Si

结构：[Li]N(C)CCN(C)C
HCID178506926

未命名化合物

PRODUCTS

生成物

1
结构：CC[Si](CC)(CC)c1cc(C=O)c(-c2ccccc2)o1
HCID19433144

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl-].[Cl-].[Zn+2]
催化剂HCID3007855

Zinc chloride

Cl2Zn

结构：[Pd].c1ccc(P(c2ccccc2)c2ccccc2)cc1.c1ccc(P(c2ccccc2)c2ccccc2)cc1.c1ccc(P(c2ccccc2)c2ccccc2)cc1.c1ccc(P(c2ccccc2)c2ccccc2)cc1
催化剂HCID11979704

未命名化合物

PROCEDURE

实验过程

Treatment of 2-triethylsilyl-4-furaldehyde with lithio N,N,N'-trimethylethylenediamine, followed by phenyl trifluoromethanesulfonate in the presence of anhydrous zinc chloride and tetrakis (triphenylphosphine) palladium (o) and work up gives the titled aldehyde.