化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 2-[(2-methoxy-2-oxoethyl)amino]acetate → N-(2-methoxy-2-oxoethyl)-N-[3-(tetradecyloxy)benzoyl]glycine methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 2-[(2-methoxy-2-oxoethyl)amino]acetate | HCID 428827 | — |
| 反応物 | 3-(Tetradecyloxy)benzoic acid | HCID 3262311 | — |
| 生成物 | N-(2-methoxy-2-oxoethyl)-N-[3-(tetradecyloxy)benzoyl]glycine methyl ester | HCID 19091823 | — |
反応手順
The conversion of 3-(tetradecyloxy)benzoic acid to the acid chloride followed by treatment with dimethyl iminodiacetate as in Example 1 gave N-(2-methoxy-2-oxoethyl)-N-[3-(tetradecyloxy)benzoyl]glycine methyl ester, mp <23°. The nmr and mass spectra were consistent with the structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05298652 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-3d931b572aa443c49df484eedc17664f |
| 出典メモ | uspto-grants-1994_03 |