HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristyl bromide → HCID 86747714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristyl bromide | HCID 8208 | — |
| Reactant | Methyl Gentisate | HCID 75077 | — |
| Product | HCID 86747714 | HCID 86747714 | 43% |
Reaction Steps
The reaction of 2,5-dihydroxybenzoic acid methyl ester with 1-bromotetradecane under conditions described in Example 58 gave 2-(hydroxy-5-(tetradecyloxy)benzoic acid methyl ester (43% yield, mp 49°-53°). The nmr and mass spectra were compatible with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298652 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-ff0f6664bfac4c6fab0214043696fc92 |
| Source note | uspto-grants-1994_03 |