HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-4-ethynyl- → 2-(4-Chloro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-4-ethynyl- | HCID 70118 | — |
| Reactant | ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate | HCID 13897513 | — |
| Product | 2-(4-Chloro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester | HCID 9944246 | — |
Reaction Steps
The title compound, MS: m/e=303.0 (M+H+) was prepared in accordance with the general method of example 1b from 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester and 1-chloro-4-ethynylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972299B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-92a1f448e2844aa48f91b7bb058194b9 |
| Source note | uspto-grants-2005_12 |