HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-2-fluorobenzene → 2-(2-Fluoro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-2-fluorobenzene | HCID 643358 | — |
| Reactant | ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate | HCID 13897513 | — |
| Product | 2-(2-Fluoro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester | HCID 9878980 | — |
Reaction Steps
The title compound, MS: m/e=287.4 (M+H+) was prepared in accordance with the general method of example 1b from 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester and 1-ethynyl-2-fluorobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972299B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-056d56e89d48412eb56657fa49d3d89b |
| Source note | uspto-grants-2005_12 |