HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Nitrophenyl)acetic acid → 1,1-Dibutylamino-4-[2-(4-nitrophenyl)ethenyl]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Nitrophenyl)acetic acid | HCID 4661 | — |
| Reactant | 4-(Dibutylamino)benzaldehyde | HCID 605391 | — |
| Solvent | Piperidine | HCID 8082 | — |
| Product | 1,1-Dibutylamino-4-[2-(4-nitrophenyl)ethenyl]benzene | HCID 73879449 | 43.6% |
Reaction Steps
The title compound was prepared from p-nitrophenylacetic acid (9.92 g, 0.055 mol) and 4-dibutylamino-benzaldehyde (14.32 g, 0.055 mol) in piperidine (5 mL) using the procedure described in Example 1, Step A. This procedure yielded a red solid, 4.12 g (0.012 mol, 16%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972287B1 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-ebb2a6ba17cb47068d70c9620db413ec |
| Source note | uspto-grants-2005_12 |