1,1-Dibutylamino-4-[2-(4-nitrophenyl)ethenyl]benzene → HCID 86594891, compound

Participants

Reaction Steps

The title compound was prepared from 1,1-dibutylamino-4-[2-(4-nitrophenyl)ethenyl]benzene (4.10 g, 11.63 mmol) and Ra—Ni (2.0 g) in MeOH (100 mL) at 21° C. to 32° C. (ΔP=3.6 psi) under a hydrogen atmosphere using the procedure described in Example 1, Step B. This procedure yielded a colorless oil, 3.49 g (10.76 mmol, 92.6%) of the desired product.

Provenance & Evidence