HCID 22269747, compound → HCID 22269697, compound

Participants

Reaction Steps

The title compound was prepared from trans-1-chloro-2-trifluoromethyl-4-[2-(4-nitrophenyl)ethenyl]benzene (22.53 g, 0.069 mol) and Ra—Ni (22 g) in THF (0.5 L) at 18° C. to 29° C. (ΔP=20.5 psi) under a hydrogen atmosphere using the procedure described in Example 1, Step B. This procedure yielded a white solid, 20.0 g (66.73 mmol, 97%) of the desired product. mp 62-64° C.

Provenance & Evidence