HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethoxybiphenyl → 2,4-Dimethoxy-3-phenylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethoxybiphenyl | HCID 914257 | — |
| Reactant | 3-Chloro-2,4-dimethoxybenzaldehyde | HCID 13343705 | — |
| Product | 2,4-Dimethoxy-3-phenylbenzaldehyde | HCID 21946143 | 95% |
Reaction Steps
Compound 2c was synthesized from 1c in 95% yield using the procedure described for 2a. 1H NMR(acetone-d6): δ 10.28 (s, 1H), 7.88 (d, J=8.8 Hz, 1H), 7.42–7.49 (m, 5H), 7.10 (d, J=8.8 Hz, 1H), 3.89 (s, 3H), 3.48 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972339B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-12b2eb005fb74b858047853a45be5cd3 |
| Source note | uspto-grants-2005_12 |