HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-Phenyl-2-chloro-2-methylpropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Methyl-1-phenyl-2-propanol | HCID 7531 | — |
| Product | 1-Phenyl-2-chloro-2-methylpropane | HCID 296357 | — |
Reaction Steps
A mixture of 5.92 g (40 mmoles) of 1-phenyl-2-hydroxy-2-methylpropane and 50 mL conc. hydrochloric acid was stirred at ice bath temperature for 1 h and at RT for 3 h. The reaction mixture was then extracted with ether. The organic layer was dried over MgSO4. Solvent removal gave 1-phenyl-2-chloro-2-methylpropane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972295B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-71517d87ceb4473aa3e70aa0bb52bb35 |
| Source note | uspto-grants-2005_12 |