HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 724424-81-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Methyl-5-nitrobenzoic acid | HCID 519683 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 724424-81-1 | HCID 68656110 | — |
Reaction Steps
A slurry of 5-nitro-2-methyl-benzoic acid (17.1 g, 94.4 mmol) and 10% Pd/C (500 mg) in EtOH (500 mL) was shaken under 40 psi H2 at ambient temperature for 4 hours. HCl was added and the solution filtered through a pad of celite. The filtrate was concentrated in vacuo to give the title compound (17.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06974812B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-31a4d276b63f4f72aa97b6a34062dced |
| Source note | uspto-grants-2005_12 |