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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 488972Generated: October 26, 2026

2,5-Bis(4-(3,5,5-trimethylhexyl)benzoyl)terephthalic acid → 2,5-Bis[4-(3,5,5-trimethylhexyl)benzyl]terephthalic acid

https://huagongshe.com/reaction/488972

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,5-Bis(4-(3,5,5-trimethylhexyl)benzoyl)terephthalic acidHCID 22269437—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
Product2,5-Bis[4-(3,5,5-trimethylhexyl)benzyl]terephthalic acidHCID 22269452—

Reaction Steps

A mixture containing 20.0 grams of 2,5-bis[4-(3,5,5-trimethylhexyl)benzoyl]terephthalic acid in 1500 mL of tetrahydrofuran (THF) and 1.4 grams of 10% palladium on carbon (as a catalyst) was heated to 90° C. in an atmosphere of hydrogen at 620 kPa and 90° C. for 17 hours. The mixture was filtered through Celite™ diatomaceous earth filter agent to remove the catalyst. The filtrate was concentrated in vacuo to give 2,5-bis[4-(3,5,5-trimethylhexyl)benzyl]terephthalic acid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06974877B2
Source datasetuspto-grants-2005_12
ORD IDord-9e592d40d35b4952a3076ab487712d7a
Source noteuspto-grants-2005_12