反应详情

温度

155 °C

A mixture of 1.0 grams of 3,10-dihexylpentacene-5,12-dione and 2.5 grams of aluminum tri(sec-butoxide) in 50 mL of mesitylene was heated to 155° C. for 2 days and cooled. The reaction mixture was filtered and the residue washed with concentrated HCl to give 2,9-dihexylpentacene.

1. temperaturecooled
2. filtrationThe reaction mixture was filtered
3. washthe residue washed with concentrated HCl