HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → Styrene-butadiene-styrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | N,N,N',N'-Tetramethylethylenediamine | HCID 8037 | — |
| Reactant | CID 53628100 | HCID 178418400 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Styrene-butadiene-styrene | HCID 22280236 | — |
Reaction Steps
Styrene, butadiene and styrene were consecutively polymerized in a cyclohexane solvent in the presence of s-butyllithium and TMEDA in the same manner as in Referential Example 2, to give a styrene-butadiene-styrene block copolymer. The thus-obtained block copolymer was hydrogenated in the same manner as in Referential Example 2, to give a hydrogenated block Copolymer No. 3 (the hydrogenated block copolymer obtained in Referential Example 4 will be abbreviated as “Copolymer No. 3” hereinafter). Table 3 shows a styrene content, a number average molecular weight, a vinyl bond content and a hydrogenation ratio of the obtained Copolymer No. 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06977105B1 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-a10cc98e03f040569e844ddc88d0d4a4 |
| Source note | uspto-grants-2005_12 |