Ethyl 4,4,4-trifluoroacetoacetate → HCID 178469135, compound

HRID 489322Notes

Reaction equation

HRID 489322 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:13]=[CH:12][C:9]([CH:10]=O)=[CH:8][CH:7]=1)=[O:5])[CH3:2].[NH2:14][C:15]1[CH:19]=[CH:18][NH:17][N:16]=1.[F:20][C:21]([F:31])([F:30])[C:22](=O)[CH2:23][C:24]([O:26][CH2:27][CH3:28])=[O:25]>>[CH2:1]([O:3][C:4]([C:6]1[CH:13]=[CH:12][C:9]([CH:10]2[C:23]([C:24]([O:26][CH2:27][CH3:28])=[O:25])=[C:22]([C:21]([F:20])([F:30])[F:31])[NH:14][C:15]3=[N:16][NH:17][CH:18]=[C:19]23)=[CH:8][CH:7]=1)=[O:5])[CH3:2]

Participants

4

Reactant 3

HCID 67793Ethyl 4,4,4-trifluoroacetoacetateHCID 80498Ethyl 4-formylbenzoateHCID 178418806HCID 178418806, compound

Product 1

HCID 178469135HCID 178469135, compound

Procedure

The title compound was prepared from 4-ethoxycarbonylbenzaldehyde, 3-aminopyrazole and ethyl trifluoroacetoacetate in the same manner as in Example 1.

Sources & evidence

ORD record
ord-88e913ce28664905a28ec99149771f25
Source dataset
uspto-grants-2005_12
Patent number
US06977262B2

Reaction notes

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