HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate → 2-(2,6-Dichloro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate | HCID 13897513 | — |
| Reactant | Benzene, 1,3-dichloro-2-ethynyl- | HCID 22271730 | — |
| Product | 2-(2,6-Dichloro-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester | HCID 9945730 | — |
Reaction Steps
The title compound, MS: m/e=197.4 (M+H+) was prepared in accordance with the general method of example 1b from 1,3-dichloro-2-ethynyl-benzene and 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706707B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-10165ae160ae40ec93690a7692d24e2b |
| Source note | uspto-grants-2004_03 |