1,4'-Bipiperidine → HCID 22263081, compound

HRID 489911Notes

Reaction equation

HRID 489911 reaction equation
[N:1]1([CH:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:13]1[C:26]2[C:17](=[CH:18][C:19]3[C:24]([C:25]=2[C:27](Cl)=[O:28])=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH:16]=[CH:15][CH:14]=1>>[CH:23]1[C:24]2[C:19](=[CH:18][C:17]3[C:26]([C:25]=2[C:27]([N:10]2[CH2:11][CH2:12][CH:7]([N:1]4[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]4)[CH2:8][CH2:9]2)=[O:28])=[CH:13][CH:14]=[CH:15][CH:16]=3)[CH:20]=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 786071,4'-BipiperidineHCID 167528Anthracene-9-carbonyl chloride2×

Product 1

HCID 22263081HCID 22263081, compound

Procedure

Anthracen-9-yl-[1,4′]bipiperidinyl-1′-yl-methanone was prepared as a pale yellow powder from 4-piperidinopiperidine and anthracene-9-carbonyl chloride (Intermediate 3) by a procedure analogous to that described above for the preparation of Example 127.

Workup

  1. customthat described above for the preparation of Example 127

Sources & evidence

ORD record
ord-a1991ada84e1492a95afd5ca99f7304b
Source dataset
uspto-grants-2005_12
Patent number
US06979741B2

Reaction notes

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