N-BOC-ethylenediamine → HCID 87598284, compound

HRID 490228Notes

Reaction equation

HRID 490228 reaction equation
CO[C:3](=[C:10]([C:13]#[N:14])[C:11]#[N:12])[C:4]1[N:5]([CH3:9])[CH:6]=[CH:7][CH:8]=1.[NH2:15][CH2:16][CH2:17][NH:18][C:19](=[O:25])[O:20][C:21]([CH3:24])([CH3:23])[CH3:22]>>[C:13]([C:10]([C:11]#[N:12])=[C:3]([NH:15][CH2:16][CH2:17][NH:18][C:19]([O:20][C:21]([CH3:24])([CH3:23])[CH3:22])=[O:25])[C:4]1[N:5]([CH3:9])[CH:6]=[CH:7][CH:8]=1)#[N:14]

Participants

3

Reactant 2

HCID 187201N-BOC-ethylenediamineHCID 23033056HCID 23033056, compound

Product 1

HCID 87598284HCID 87598284, compound

Procedure

N-(2-{[2,2-dicyano-1-(1-methylpyrrol-2-yl)vinyl]amino}ethyl)(tert-butoxy)carboxamide was synthesized in the same manner using [methoxy(1-methylpyrrol-2-yl)methylene]methane-1,1-dicarbonitrile and tert-butyl N-(2-aminoethyl)carbamate. The ESI/MS data for this compound are shown below.

Sources & evidence

ORD record
ord-95fffee217104e06bc5b45a8d99e0b9a
Source dataset
uspto-grants-2009_05
Patent number
US07528140B2

Reaction notes

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