反应详情

A solution of D3 (2.01 g, 9.94 mM) and 10% palladium on charcoal (1 g) in methanol was hydrogenated at atmospheric pressure for 1 h. The catalyst was filtered off and the filtrate concentrated under reduced pressure to afford the product as a cream coloured solid.

1. filtrationThe catalyst was filtered off
2. concentrationthe filtrate concentrated under reduced pressure
3. customto afford the product as a cream