HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)phenylboronic acid → 4-(4'-Dimethylamino-biphenyl-4-yloxymethyl)-5-methyl-furan-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)phenylboronic acid | HCID 2734344 | — |
| Reactant | 4-(4-Iodo-phenoxymethyl)-5-methyl-furan-2-carboxylic acid | HCID 18444654 | — |
| Product | 4-(4'-Dimethylamino-biphenyl-4-yloxymethyl)-5-methyl-furan-2-carboxylic acid | HCID 18444569 | — |
Reaction Steps
Compound (113) was prepared from compound (26) and (4-dimethylamino-phenyl)-boronic acid by adapting the procedure of Example 27B. LC/MS System B; Rt=1.83 mins, m/z (ES−)=350 (M−H for C21H21NO4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528157B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-ba0ba2f0fdab46c998e3b34c1e90e920 |
| Source note | uspto-grants-2009_05 |