1-Bromo-2,4-dimethoxybenzene → HCID 58824171, compound

HRID 490390Notes

Reaction equation

HRID 490390 reaction equation
[CH3:1][O:2][C:3]([C:5]1[O:6][C:7]([CH3:27])=[C:8]([CH2:10][O:11][C:12]2[CH:17]=[CH:16][C:15](B3OC(C)(C)C(C)(C)O3)=[CH:14][CH:13]=2)[CH:9]=1)=[O:4].Br[C:29]1[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[CH:31][C:30]=1[O:37][CH3:38]>>[CH3:1][O:2][C:3]([C:5]1[O:6][C:7]([CH3:27])=[C:8]([CH2:10][O:11][C:12]2[CH:13]=[CH:14][C:15]([C:29]3[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[CH:31][C:30]=3[O:37][CH3:38])=[CH:16][CH:17]=2)[CH:9]=1)=[O:4]

Participants

3

Reactant 2

HCID 872661-Bromo-2,4-dimethoxybenzeneHCID 588241625-Methyl-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxymethyl]-furan-2-carboxylic acid methyl ester

Product 1

HCID 58824171HCID 58824171, compound

Procedure

Compound (139) was prepared from compound (119) and 1-bromo-2,4-dimethoxy-benzene by adapting the procedure of Example 31(a). LC/MS System A; Rt=4.09 mins.

Sources & evidence

ORD record
ord-975c0ff09752422280393a827607afef
Source dataset
uspto-grants-2009_05
Patent number
US07528157B2

Reaction notes

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