HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazin-2-one → HCID 11546815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazin-2-one | HCID 4399042 | — |
| Reactant | HCID 9903065 | HCID 9903065 | — |
| Product | HCID 11546815 | HCID 11546815 | 69.1% |
Reaction Steps
4-{[5,6-Dimethoxy-3-(1H-pyrrolo[2,3-b]pyridin-2-yl)-indol-1-yl]acetyl}-1-methylpiperazin-2-one is prepared by following the procedure described in example 93, but using 0.1 g of 2-[5,6-dimethoxy-3-(1H-pyrrolo[2,3-b]pyridin-2-yl)indol-1-yl]acetic acid and 0.039 g of 1-methylpiperazin-2-one. 0.088 g of 4-{[5,6-dimethoxy-3-(1H-pyrrolo[2,3-b]pyridin-2-yl)indol-1-yl]acetyl}-1-methylpiperazin-2-one is obtained, the characteristics of which are as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528147B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-401f2aaaf1bc4dbab9e6b2cd564181b7 |
| Source note | uspto-grants-2009_05 |