HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4'-Bipiperidine → HCID 67147489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4'-Bipiperidine | HCID 78607 | — |
| Reactant | HCID 67147672 | HCID 67147672 | — |
| Product | HCID 67147489 | HCID 67147489 | 97.6% |
Reaction Steps
4-Chloro-2-[1-methyl-5-methoxy-6-(2-(4-piperidylpiperidin-1-yl)ethoxy)-1H-indol-3-yl]-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridine is prepared by following the procedure described in example 147b, but using 0.212 g of 4-piperidinopiperidine and 0.400 g of 4-chloro-2-[1-methyl-5-methoxy-6-(2-iodoethoxy)-1H-indol-3-yl]-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridine. 0.415 g of 4-chloro-2-[1-methyl-5-methoxy-6-(2-(4-piperidylpiperidin-1-yl)ethoxy)-1H-indol-3-yl]-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridine is obtained, the characteristics of which are as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528147B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-4c5aeb14c7704d9bb0a09573fb823d95 |
| Source note | uspto-grants-2009_05 |