HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoyl chloride → HCID 25121362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | HCID 57674252 | HCID 57674252 | — |
| Product | HCID 25121362 | HCID 25121362 | 7.7% |
Reaction Steps
As described for Example 89e, 2-[4-(4-amino-1-benzyl-pyrrolidine-2-carbonyl)-piperazin-1-yl]-benzonitrile (50.0 mg, 0.128 mmol) was converted, using 2-methoxy-benzoyl chloride instead of 2-chloro-benzoyl chloride, to the title compound (5.2 mg, 7.7%) as light yellow oil. MS m/e=524.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528136B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-36844f18e5df42e3b91e3a98f5da2a26 |
| Source note | uspto-grants-2009_05 |