HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)thiobenzamide → HCID 69056994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)thiobenzamide | HCID 2734823 | — |
| Reactant | HCID 85860554 | HCID 85860554 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69056994 | HCID 69056994 | — |
Reaction Steps
A mixture of 4-Trifluoromethyl-thiobenzamide (12.3 g, 60 mmol) and the crude product from step A (16.6 g, 66 mmol) in ethanol (600 mL) is heated to reflux for 3 days. Solvent is evaporated and the residue is purified by chromatography on silica gel yielding the title compounds (14.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528160B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-e8bb084c92a64058b57914cad0b156eb |
| Source note | uspto-grants-2009_05 |