4-Methoxyphenylacetic Acid → HCID 57675201, compound

HRID 490921Notes

Reaction equation

HRID 490921 reaction equation
[CH2:1]([N:3]1[C:7]2=[N:8][CH:9]=[C:10]([C:19](=[NH:22])[NH:20][OH:21])[C:11]([NH:12][CH:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)=[C:6]2[CH:5]=[N:4]1)[CH3:2].[CH3:23][O:24][C:25]1[CH:30]=[CH:29][C:28]([CH2:31][C:32](O)=O)=[CH:27][CH:26]=1>>[CH2:1]([N:3]1[C:7]2[N:8]=[CH:9][C:10]([C:19]3[N:22]=[C:32]([CH2:31][C:28]4[CH:29]=[CH:30][C:25]([O:24][CH3:23])=[CH:26][CH:27]=4)[O:21][N:20]=3)=[C:11]([NH:12][CH:13]3[CH2:14][CH2:15][O:16][CH2:17][CH2:18]3)[C:6]=2[CH:5]=[N:4]1)[CH3:2]

Participants

3

Reactant 2

HCID 76904-Methoxyphenylacetic AcidHCID 178463012HCID 178463012, compound

Product 1

HCID 57675201HCID 57675201, compound

Procedure

Prepared from Intermediate 138 and 4-methoxyphenylacetic acid using a similar process to that described for Example 189 using similar or the same number of moles of reagents and/or volumes of solvents. LCMS showed MH+=435; TRET=3.26 min

Workup

  1. customTRET=3.26 min

Sources & evidence

ORD record
ord-459978c097124f989a86bf11eab05f1c
Source dataset
uspto-grants-2009_05
Patent number
US07528148B2

Reaction notes

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