huagongshe.com
HRID4911

反应详情

EQUATION

反应方程式

HRID 4911 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccccc1CBr
HCID6992

1-(Bromomethyl)-2-methylbenzene

C8H9Br

结构：CC(C)OP(OC(C)C)OC(C)C
HCID8304

Tripropan-2-yl phosphite

C9H21O3P

PRODUCTS

生成物

1
结构：Cc1ccccc1CP(=O)(OC(C)C)OC(C)C
HCID15166402

未命名化合物

PROCEDURE

实验过程

34.5 g (0.19 mol) of 2-methylbenzyl bromide and 39 g (0.19 mol) of triisopropyl phosphite were heated at 150° C. for 2 hours. During this procedure, i-propyl bromide distilled off. The product was distilled through a 30 cm Vigreux column.

WORKUP

后处理

  1. distillationDuring this procedure, i-propyl bromide distilled off
  2. distillationThe product was distilled through a 30 cm Vigreux column