HCID 68841076, compound → HCID 57678248, compound

Participants

Reaction Steps

Benzyl 4-(6-methoxypyridin-3-yl)-2,3-dihydro-1H-pyrrole-1-carboxylate (100 mg, 0.33 mmol) was dissolved in methanol (10 mL). The solution was purged with nitrogen for 10 minutes and then treated with 5% Pd/C (10 mg). The reaction was stirred under a hydrogen atmosphere overnight. The catalyst was filtered off and the filtrate was concentrated to provide the title compound (60 mg, 95%). 1HNMR (500 MHz, CDCl3) δ 8.03 (m, 1H), 7.50 (m, 1H), 6.66 (m, 1H), 3.86 (s, 3H), 3.22 (m, 2H), 3.01 (m, 2H), 2.67 (m, 1H), 2.32 (m, 1H), 1.70 (m, 1H).

Provenance & Evidence