HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dibromoethane → HCID 178419616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dibromoethane | HCID 11201 | — |
| Reactant | 5-Bromo-1-benzothiophene | HCID 2776578 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178419616 | HCID 178419616 | — |
Reaction Steps
A solution of magnesium (34 mg, WAKO) in dehydrated THF (0.7 ml) was added dropwise with a solution of 5-bromobenzo[b]thiophene (149.2 mg, MAYB) and dibromoethane (30 μl, WAKO) in dehydrated THF (0.7 ml) under an argon atmosphere, and the mixture was stirred at room temperature for 2 hours to obtain a THF solution of the title compound (Compound No. MG01).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531533B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-9de729cfa601417596700dc5f6e8366f |
| Source note | uspto-grants-2009_05 |