Picolyl chloride hydrochloride → HCID 68876783, compound

HRID 491453Notes

Reaction equation

HRID 491453 reaction equation
[ClH:1].[N:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][Cl:9].Cl.[CH3:11][O:12][C:13]1[CH:14]=[C:15]([C:21]2[C@@H:30]3[C@@H:25]([CH2:26][CH:27]=[CH:28][CH2:29]3)[C:24](=[O:31])[N:23]([CH:32]3[CH2:37][CH2:36][N:35](CC4C=C5C(C=CC(=O)O5)=CC=4)[CH2:34][CH2:33]3)[N:22]=2)[CH:16]=[CH:17][C:18]=1[O:19][CH3:20]>>[ClH:9].[ClH:1].[CH3:11][O:12][C:13]1[CH:14]=[C:15]([C:21]2[C@@H:30]3[C@@H:25]([CH2:26][CH:27]=[CH:28][CH2:29]3)[C:24](=[O:31])[N:23]([CH:32]3[CH2:37][CH2:36][N:35]([CH2:8][C:3]4[CH:4]=[CH:5][CH:6]=[CH:7][N:2]=4)[CH2:34][CH2:33]3)[N:22]=2)[CH:16]=[CH:17][C:18]=1[O:19][CH3:20]

Participants

3

Reactant 2

HCID 23392Picolyl chloride hydrochlorideHCID 86601097HCID 86601097, compound

Product 1

HCID 68876783HCID 68876783, compound

Procedure

Prepared from compound A1 and 2-picolylchloride hydrochloride as described for compound 18. M.p. 214-216° C.

Sources & evidence

ORD record
ord-ecc1248501bc4f988dd1612bc76d8b73
Source dataset
uspto-grants-2009_05
Patent number
US07531540B2

Reaction notes

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