p-Anisoyl chloride → HCID 135495079, compound

HRID 491724Notes

Reaction equation

HRID 491724 reaction equation
[Cl:1][C:2]1[C:3]([O:11]C)=[CH:4][C:5]([O:9][CH3:10])=[C:6]([CH:8]=1)[NH2:7].C[O:14][C:15]1[CH:23]=[CH:22][C:18](C(Cl)=O)=[CH:17][CH:16]=1>>[Cl:1][C:2]1[C:3]([OH:11])=[CH:4][C:5]2[O:9][C:10]([C:18]3[CH:22]=[CH:23][C:15]([OH:14])=[CH:16][CH:17]=3)=[N:7][C:6]=2[CH:8]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 668075-Chloro-2,4-dimethoxyaniline

Product 1

HCID 135495079HCID 135495079, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 16, from 5-chloro-2,4-dimethoxyaniline, and 4-methoxybenzoyl chloride and was obtained as an off-white solid, m.p. 254-256° C.; MS m/e 262 (M+H)+.

Workup

  1. customwas obtained as an off-white solid, m.p. 254-256° C.

Sources & evidence

ORD record
ord-f86e710b74874f589c2a0234db956810
Source dataset
uspto-grants-2009_05
Patent number
US07531564B2

Reaction notes

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