huagongshe.com
HRID49176

反应详情

EQUATION

反应方程式

HRID 49176 的结构方程式

REACTANTS

反应物

2
结构：COCCS(N)(F)(F)(F)CCOC
HCID53904438

未命名化合物

结构：CN1[C@@H]2CC=C[C@@]1(OC(=O)C(O)(c1ccc(F)cc1)c1ccc(F)cc1)CC2
HCID86585677

未命名化合物

PRODUCTS

生成物

1
结构：CN1[C@@H]2CC=C[C@@]1(O)CC2.O=C([O-])C(F)(c1ccc(F)cc1)c1ccc(F)cc1
HCID86585678

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

2.94 g (0.013 mol) of bis-(2-methoxyethyl)-aminosulphur trifluoride are reacted with 3.85 g (0.01 mol) of 5d analogously to Example 4, step 4.3 in 100 ml of dichloromethane. The product is recrystallised from acetonitrile in the form of its hydrochloride.

WORKUP

后处理

  1. customThe product is recrystallised from acetonitrile in the form of its hydrochloride