Triethylamine → HCID 68886565, compound

Participants

Reaction Steps

Compound #152 (0.115 g, 0.24 mmol), prepared, for example, as described in Example 44 above, was taken up into DCM (5 mL) and then triethylamine (34 μL, 0.24 mmol) was added. Methoxy-acetyl chloride (22 μL, 0.24 mmol) was added, and the reaction mixture was stirred at room temperature overnight. The reaction mixture was purified using normal phase chromatography (heptanes:EtOAc) to yield the title compound as a white powder.

Provenance & Evidence