HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(4-aminophenyl)acrylate → Ethyl 3-(4-aminophenyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(4-aminophenyl)acrylate | HCID 97826 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(4-aminophenyl)propanoate | HCID 10442595 | 99% |
Reaction Steps
A mixture of ethyl 3-(4-aminophenyl)acrylate (1.5 g) and 10% Pd on activated carbon (0.3 g) in ethanol (20 ml) was hydrogenated at 30 psi for 18 h and filtered over Celite. Removal of the volatiles in vacuo provided ethyl 3-(4-aminophenyl)propionate (1.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531566B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-94bf571d59d14edd8908fb2076276136 |
| Source note | uspto-grants-2009_05 |