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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 492100Generated: November 2, 2026

Triethylamine → HCID 66593512, compound

https://huagongshe.com/reaction/492100

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantPivaloyl chlorideHCID 62493—
ReactantHCID 66593931HCID 66593931—
ProductHCID 66593512HCID 6659351289%

Reaction Steps

0.534 g of (2.68 mmol) of 2-(2,3,5-trimethylcyclopenta-1,4-dienyl)phenylamine, 0.325 g (3.22 mmol) of triethylamine, and 0.388 g (3.22 mmol) of pivaloyl chloride were used in the same manner as in Example 11. The resultant reaction product was purified through a column chromatography using a hexane/ethyl acetate (v/v, 5:1) solvent, and then the solvent in the purified product was removed in vacuum, thereby obtaining white solid (0.674 g, 89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07531608B2
Source datasetuspto-grants-2009_05
ORD IDord-69977201c00e4630822c409f401efc31
Source noteuspto-grants-2009_05