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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 492654Generated: October 27, 2026

Methane → Divinylbenzene-styrene

https://huagongshe.com/reaction/492654

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethaneHCID 297—
ReactantStyreneHCID 7501—
Reactant1,2-DiethenylbenzeneHCID 66666—
ReactantLauryl peroxideHCID 76169—
ReactantHCID 178508066HCID 178508066—
SolventWaterHCID 962—
ProductDivinylbenzene-styreneHCID 174664—

Reaction Steps

The positively charged black color particles for display media were produced as follows. 3 parts by weight of nigrosine compound (Bontoron N07: product of Orient Chemical Industries, Ltd.) as a positive charge control agent, and, 5 parts by weight of carbon black (SPECIAL BLACK 5: production of Degussa) as black pigment were dispersed by a sand mill in 94 parts by weight of styrene monomer (KANTO CHEMICAL CO., INC.) and 6 parts by weight of divinylbenzen (KANTO CHEMICAL CO., INC.), and then 2 parts by weight of lauryl peroxide (PEROYL L: product of NOF CORPORATION) was further dissolved therein so as to obtain a liquid. The thus obtained liquid was suspended and polymerized in a purified water in which 0.5% of polyoxyethylene ether sodium sulfate (LATEMURU E-118B: product of KAO CORPORATION) as a surface active agent was added, and then the thus polymerized liquid was subjected to a filtering and drying process. Then, the particles 1 having a particle diameter range of 0.1-50 μm and an average particle diameter of 10 μm were obtained by classifying the dried member by means of classifier (MDS-2: NIPPON PNEUMATIC MFG. CO., LTD.). A glass transition temperature Tg measured by DSC measurement method was 75° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07532387B2
Source datasetuspto-grants-2009_05
ORD IDord-c53f51291c334833a6cdb2909a9f4b4a
Source noteuspto-grants-2009_05