HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Triethoxyaniline → 3,5-Dimethoxy-4-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Triethoxyaniline | HCID 18630560 | — |
| Reactant | 3,4,5-Triethoxy-1-iodobenzene | HCID 22933075 | — |
| Product | 3,5-Dimethoxy-4-methylaniline | HCID 12752288 | — |
Reaction Steps
Following the procedure of the synthesis of 3,4,5-triethoxy-1-iodobenzene from the oil containing 3,4,5-triethoxyaniline in Reference Example 5,1-iodo-3,5-dimethoxy-4-methylbenzene was obtained as a pale yellow amorphous powder (7.59 g, yield: 87%) from 3,5-dimethoxy-4-methylaniline (J. Chem. Soc., 497-506 (1963)) (5.23 g, 31.3 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706703B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-eea9413aca02405fac9057aca84b93bd |
| Source note | uspto-grants-2004_03 |